Skalar analytical equipment generally operates on principles of continuous flow analysis (CFA), high-temperature combustion, and detection methods like infrared and thermal conductivity. These instruments are used for analyzing various parameters in different types of samples like water, soil, and solid materials.
Here's a more detailed look at some key principles:
1. Continuous Flow Analysis (CFA):
Principle: Samples are carried through a system of tubes and reactors where they react with reagents, and the resulting products are measured by a detector.
Applications: Skalar SAN analyzers for total nitrogen and total phosphorus in various water types.
Benefits: Automated, efficient, and suitable for a wide range of samples.
2. High-Temperature Combustion:
Principle:
Samples are heated to high temperatures to convert organic compounds into gases that can be detected.
Applications:
PRIMACS™ series for total carbon and total nitrogen analysis in solid samples.
Methods:
Dumas methodology for nitrogen analysis and infrared detection for carbon analysis.
3. Detection Methods:
Non-Dispersive Infrared (NDIR) Detection: Measures carbon dioxide produced during combustion or acidification.
Thermal Conductivity Detection (TCD): Measures the amount of nitrogen gas produced after reduction of nitrogen oxides.
Photo-Multiplier Tube (PMT) Detection: Detects photons emitted in chemical reactions, such as the reaction between nitrogen and ozone.
4. Sample Preparation and Handling:
In-line sample preparation:
Many Skalar analyzers offer automated sample preparation steps like UV-digestion, distillation, extraction, dialysis, and ion-exchange.
Automated sample introduction:
PRIMACS™ SNC-100 analyzers use a unique vertical "bottom-to-top" system for introducing samples into the combustion furnace.
Sample handling systems:
SP2000 robotic analyzers and other systems automate sample handling, including sample preparation, pipetting, titration, and photometric detection.
5. Software and Automation:
FlowAccess software: Controls the entire analyzer, including start-up, function control, autoscaling, and result processing.
Automated standards creation: Skalar samplers offer automatic standards creation and reagent addition.
High-throughput analysis: SP2000 robotic analyzers are designed for high-throughput analytical testing, automating processes like sample preparation and detection.
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